12 Hardware Information This chapter describes the autosampler in more detail on hardware and electronics.Ĭontents Contents 1 Introduction 9 Features 10 Overview of the Module 11 Autosampler Principle 13 System Overview 19 2 Site Requirements and Specifications 23 Site Requirements 24 Physical Specifications 27 Specifications 28 3 Installing the Autosampler 31 Unpacking the Autosampler 32 Optimizing the Stack Configuration 35 Installation Information on Leak and Waste Handling Installing the Autosampler 44 Flow Connections to the Autosampler 46 4 Using the Module 40 47 Leak and Waste Handling 48 PrepĬontents 6 Troubleshooting and Diagnostics 79 Overview of the Module’s Indicators and Test Functions Status Indicators 81 User Interfaces 83 Agilent Lab Advisor Software 84 7 Error Information 80 85 What are Error Messages 87 General Error Messages 88 Module Error Messages 93 8 Test Functions 105 Introduction 106 System Pressure Test 107 Sample Transport Self Alignment Maintenance Positions 112 Injector Steps 116 9 Maintenance 110 119 Introduction to Maintenance 120 Warnings and Cautions 121 OverĬontents 10 Parts for Maintenance 145 Overview of Maintenance Parts 146 Vial Trays 147 Recommended Plates and Closing Mats Recommended Vial Plates 149 Kits 150 Analytical Head Assembly 151 Injection Valve Assembly 152 Cover Parts 153 Leak System Parts 154 11 Identifying Cables 148 155 Cable Overview 156 Analog Cables 158 Remote Cables 160 BCD Cables 163 CAN/LAN Cables 165 External Contact Cable 166 Agilent Module to PC 167 Agilent 1200 Module to Printer 12 Hardware Information 168 169 Firmware DescĬontents 14 Appendix 193 General Safety Information 194 Lithium Batteries Information 197 The Waste Electrical and Electronic Equipment (WEEE) Directive (2002/96/EC) 198 Radio Interference 199 Sound Emission 200 Use of Solvents 201 Agilent Technologies on Internet 202 8 Agilent 1260 Infinity High Performance Autosampler User ManualĪgilent 1260 Infinity High Performance Autosampler User Manual 1 Introduction Features 10 Overview of the Module Autosampler Principle 11 13 System Overview 19 Leak and Waste Handling 19 This chapter gives an introduction to the autosampler.ġ Introduction Features Features The 1260 Infinity High Performance Autosampler features an increased pressure range (up to 600 bar) enabling the use of today’s column technology (sub- two- micron narrow bore columns) with the Agilent 1260 Infinity Binary LC System.
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11 Identifying Cables This chapter provides information on cables used with the Agilent 1200 Infinity Series modules. 9 Maintenance This chapter describes the maintenance of the Autosampler 10 Parts for Maintenance This chapter provides information on parts material required for the module. In This Guide 8 Test Functions This chapter describes the tests for the module. 3 Installing the Autosampler This chapter provides information on unpacking, checking on completeness, stack considerations and installation of the autosampler. 2 Site Requirements and Specifications This chapter provides information on environmental requirements, physical and performance specifications. In This Guide In This Guide This manual covers the Agilent 1260 Infinity High Performance Autosampler (G1367E) 1 Introduction This chapter gives an introduction to the autosampler.
as governed by United States and international copyright laws. 2010-2013, 2014 No part of this manual may be reproduced in any form or by any means (including electronic storage and retrieval or translation into a foreign language) without prior agreement and written consent from Agilent Technologies, Inc. Therefore, this method potentially improves the measurement of trace odourants in complex matrices by increasing specificity and sensitivity.Agilent 1260 Infinity High Performance Autosampler User Manual Agilent Technologies Optimal low EI GC-QTOF parameters (EI energy: 15 eV, acquisition rate: 3 Hz) were applied to achieve improved molecular ion signal intensity and reproducibility (relative standard deviation < 10%) across five compounds, which resulted in good linearity (R 2 ≥ 0.999) and lowered detection levels (e.g. This prompted the application of low energy electron ionisation (EI) coupled with GC-quadrupole time-of-flight (GC-QTOF). Due to matrix complexity, some trace odourants were detected in SAFE extracts by aroma extract dilution analysis (AEDA) but remained difficult to quantify by gas chromatography-mass spectrometry (GC–MS). In this study, their volatiles were extracted using solvent-assisted flavour evaporation (SAFE) and headspace solid-phase microextraction (HS-SPME). Four Arabica coffees (Brazil, Colombia, Ethiopia, and Guatemala) yield highly variant odours, attesting to the complexities of coffee aroma that command advanced analytical tools.
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